Table 4 Volume percentage of elements originally present on the untreated surface and elements which appear after instrumentation
(n = 5 spots/disc and tip) | Ti | Zr | O | C | fe % | te |
|---|---|---|---|---|---|---|
Disc I | ||||||
0 | 88.0 ± 13.6 | 0 | 5.4 ± 4.8 | 6.1 ± 8.5 | Al 9.9 | Ca, Si |
A | 83.0 ± 16.2 | 0 | 6.4 ± 2.1 | 1.5 ± 0.2 | Fe 39.1, Cr 5.4 | - |
B | 80.7 ± 18.3 | 0 | 9.3 ± 5.1 | 9.6 ± 15.3 | - | Al, Ca, Si, Fe |
C | 86.1 ± 8.6 | 0 | 10.5 ± 5.8 | 3.1 ± 2.6 | - | Si, Ca |
D | 78.1 ± 24.0 | 0 | 18.1 ± 20.5 | 12.0 ± 18.3 | S 8, Ca 3 | - |
E | 63.1 ± 31.7 | 0 | 7.2 ± 4.3 | 27.7 ± 26.5 | S 6 | Ca |
Disc II | ||||||
0 | 73.3 ± 11.5 | 12.9 ± 2.9 | 9.2 ± 9.2 | 8.7 ± 11.1 | - | S, Ca |
A | 56.5 ± 6.6 | 12.6 ± 0.4 | 8.3 ± 5.2 | 1.9 ± 0.7 | - | - |
B | 71.0 ± 15.8 | 12.1 ± 3.3 | 8.1 ± 6.3 | 8.3 ± 11.7 | - | Ca, Al, S, Na, Si |
C | 78.2 ± 4.5 | 13.3 ± 0.7 | 6.8 ± 3.7 | 1.7 ± 0.9 | - | - |
D | 62.3 ± 30.9 | 10.9 ± 5.5 | 6.2 ± 2.0 | 14.6 ± 24.2 | - | - |
E | 38.1 ± 35.7 | 6.9 ± 6.6 | 6.2 ± 4.9 | 44.2 ± 33.6 | S 14.0 | Si, Ca |
Disc III | ||||||
0 | 74.7 ± 16.7 | 0 | 16.5 ± 9.5 | 2.7 ± 1.5 | Al 27 | Ca, Si |
A | 84.6 ± 9.9 | 0 | 9.0 ± 4.0 | 1.9 ± 0.7 | Fe 9.8, Al 10.3, Cr 1.5 | - |
B | 73.7 ± 19.2 | 0 | 10.8 ± 4.6 | 12.6 ± 15.2 | Al 9.5 | Ca, Si |
C | 88.5 ± 5.1 | 0 | 8.8 ± 4.0 | 1.9 ± 0.5 | Al 5.7, | Si |
D | 58.1 ± 17.7 | 0 | 19.4 ± 10.3 | 12.8 ± 15.9 | S 13, Ca 12, Al 5, Si 2.0 | - |
E | 44.2 ± 35.4 | 0 | 17.9 ± 10.5 | 21.4 ± 23.3 | Al 51, S 6 | Ca, Na, Si |
Disc IV | ||||||
0 | 77.7 ± 2.7 | 13.9 ± 1.9 | 7.1 ± 10.2 | 3.3 ± 1.4 | - | - |
A | 78.8 ± 5.3 | 12.3 ± 2.2 | 6.0 ± 3.7 | 1.7 ± 1.6 | Fe 3.2 | - |
B | 79.4 ± 2.2 | 12.9 ± 0.8 | 5.4 ± 2.1 | 2.3 ± 0.5 | - | - |
C | 77.0 ± 4.9 | 14.5 ± 2.8 | 5.2 ± 1.7 | 3.1 ± 1.6 | - | Fe, Ca |
D | 77.4 ± 3.5 | 12.9 ± 1.2 | 7.3 ± 3.3 | 2.4 ± 1.0 | - | - |
E | 73.0 ± 13.4 | 35.0 ± 44.2 | 3.9 ± 0.5 | 7.6 ± 9.7 | - | Ca, S, B |