Monomer | Material | Fluoride application | Immersion time-periods | p* | |||
---|---|---|---|---|---|---|---|
10 min | 1 h | 24 h | 30d | ||||
TEGDMA | FBF | Control | 0.384 (0.07–0.87) | 1.083 (0.59–1.333) | 0.908 (0.28–0.29) | 0.978 (0.24–1.33) | 0.392 |
APF | 1.397 (0.16–2.10) | 0.699 (0.31–0.38) | 0.210 (0.04–1.15) | 0.699 (0.24–1.50) | 0.050 | ||
NaF | 0.035 (0.00–1.47) | 0.599 (0.21–1.36) | 0.733 (0.42–1.68) | 0.524 (0.38–0.87) | 0.145 | ||
p | 0.049 | 0.443 | 0.305 | 0.555 | |||
DXP | Control | 2.305 (0.00–3.95) | 4.121 (1.75–5.03)1 | 5.064 (0.00–8.66) | 3.982 (2.20–5.06) | 0.095 | |
APF | 2.375 (1.26–7.09) | 1.432 (1.01–2.34)2 | 4.331 (2.62–6.95) | 1.991(1.68–4.16) | 0.251 | ||
NaF | 1.013 (0.59–1.61)b | 1.257 (0.87–1.47)2.b | 3.143 (2.17–3.77)a | 1.816 (1.08–2.59)b | 0.004 | ||
p | 0.168 | 0.001 | 0.559 | 0.025 | |||
Z550 | Control | 0.384 (0.00–1.29) | 0.105 (0.00–0.45)2 | 0.419 (0.24–0.59)2 | 0.768 (0.59–0.91)1 | 0.041 | |
APF | 0.105 (0.00–0.73) | 0.105 (0.00–0.42)2 | 0.699 (0.42–1.01)2 | 0.349 (0.24–0.56)2 | 0.054 | ||
NaF | 1.362 (0.91–11.60) | 0.768 (0.38–1.05)1 | 1.432 (0.73–1.82)1 | 0.664 (0.38–1.22)1 | 0.095 | ||
p | 0.051 | 0.001 | 0.003 | 0.016 | |||
HEMA | FBF | Control | 49.447 (9.22–223.22) | 71.769 (22.67–171.74) | 38.612 (24.97–160.60) | 42.108 (0.00–71.85) | 0.178 |
APF | 29.968 (2.04–77.49) | 13.447 (11.14–50.72) | 21.938 (17.29–53.02) | 16.828 (9.99–33.04) | 0.106 | ||
NaF | 33.003 (12.29–134.09) | 35.808 (14.60–90.29) | 53.980 (22.28–113.34) | 17.865 (8.07–93.36) | 0.178 | ||
p | 0.285 | 0.151 | 0.222 | 0.616 | |||
DXP | Control | 6.378 (4.61–9.22)1 | 11.872 (8.84–13.06) | 16.751 (8.84–21.90) | 19.978 (12.68–22.28) | 0.062 | |
APF | 12.256 (7.68–18.83)2.b | 17.712 (7.30–27.66)b | 27.317 (17.67–33.81)a | 18.403 (10.37–24.21)b | 0.003 | ||
NaF | 13.524 (10.76–18.44)2 | 22.284 (18.06–28.82) | 22.245 (8.45–36.88) | 3.458 (1.77–4.19) | 0.178 | ||
p | 0.012 | 0.024 | 0.149 | 0.602 | |||
Z550 | Control | 0.231 (0.19–3.99)2 | 0.576 (0.50–1.38) | 0.307 (0.00–0.35)2 | 0.192 (0.00–1.04) | 0.145 | |
APF | 12.026 (0.58–2.08)2 | 0.615 (0.00–1.99) | 1.037 (0.58–1.35)2 | 0.845 (0.00–1.38) | 0.145 | ||
NaF | 26.010 (12.03–38.38)1.a | 4.149 (1.69–19.36)b | 4.034 (2.61–6.76)1.b | 0.922 (0.65–1.42)b | 0.004 | ||
p | 0.0001 | 0.050 | 0.0001 | 0.077 | |||
UDMA | FBF | Control | 41.697 (21.49–143.60)a | 18.083 (9.15–99.77)b | 17.232 (10.64–68.72)b | 8.297 (5.32–27.87)b | 0.003 |
APF | 19.572 (16.81–52.33)a | 9.786 (7.02–19.57)b | 11.275 (9.15–24.89)b | 6.595 (4.04–12.34)b | 0.003 | ||
NaF | 36.591 (19.99–83.82)a | 23.189 (10.64–49.57)b | 26.380 (12.13–50.21)b | 7.446 (1.92–12.13)b | 0.002 | ||
p | 0.222 | 0.224 | 0.290 | 0.213 | |||
DXP | Control | 0.000 (0.00–0.00) | 0.000 (0.00–0.00) | 0.000 (0.00–0.00) | 0.000 (0.00–0.00) | – | |
APF | 0.000 (0.00–0.00) | 0.000 (0.00–0.00) | 0.000 (0.00–0.00) | 0.000 (0.00–0.00) | – | ||
NaF | 0.000 (0.00–0.00) | 0.000 (0.00–0.00) | 0.000 (0.00–0.00) | 0.000 (0.00–0.00) | – | ||
p | |||||||
Z550 | Control | 28.507 (22.76–36.17)a | 15.743 (14.47–19.99)2.b | 16.168 (12.34–17.02)2.b | 6.595 (5.53–7.66)2.c | 0.002 | |
APF | 34.889 (20.85–45.31)a | 12.275 (8.51–16.93)2.b | 17.445 (15.32–24.68)2.b | 7.446 (6.17–11.49)2.c | 0.004 | ||
NaF | 36.804 (19.36–115.52)b | 55.950 (16.81–95.52)1.a | 54.036 (15.96–72.33)1.a | 13.828 (8.72–15.32)1.c | 0.019 | ||
p | 0.171 | 0.015 | 0.006 | 0.0001 | |||
Bis-GMA | FBF | Control | 18.923 (10.93–60.09)a | 10.535 (6.63–44.67)b | 9.559 (6.63–37.46)b | 5.072 (3.71–15.99)b | 0.003 |
APF | 11.315 (6.83–23.41)a | 4.292 (3.71–8.78)b | 5.853 (5.07–12.88)b | 3.902 (2.93–7.41)b | 0.004 | ||
NaF | 22.435 (8.97–35.90)a | 11.315 (5.27–25.17)b | 15.412 (7.22–27.51)b | 4.682 (0.59–9.56)b | 0.002 | ||
p | 0.218 | 0.153 | 0.233 | 0.215 | |||
DXP | Control | 0.956 (0.74–1.42)b | 1.483 (1.01–11.02)a | 2.165 (1.62–3.41)a | 2.282 (1.56–3.43)a | 0.029 | |
APF | 2.146 (1.37–4.68)a | 1.385 (1.09–4.45)a | 2.712 (1.84–6.30)a | 1.092 (0.00–3.00)b | 0.018 | ||
NaF | 1.151 (0.98–3.51) | 1.366 (1.01–1.46) | 3.180 (1.95–3.84) | 1.756 (0.90–2.13) | 0.062 | ||
p | 0.106 | 0.496 | 0.423 | 0.136 | |||
Z550 | Control | 18.338 (13.07–23.02)a | 7.998 (7.61–10.14)2.b | 7.998 (7.02–8.97)2.b | 3.512 (2.93–3.71)2.c | 0.002 | |
APF | 23.800 (13.46–29.46)a | 7.355 (5.66–8.97)2.b | 8.974 (7.99–13.46)2.b | 3.902 (3.36–6.44)2.c | 0.004 | ||
NaF | 31.902 (17.17–65.55)a | 31.409 (11.32–51.11)1.a | 31.018 (10.34–41.55)1.a | 7.803 (5.07–9.36)1.b | 0.011 | ||
p | 0.057 | 0.009 | 0.004 | 0.001 |